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    ZHOU Li-ping, WANG Hua, HE Dan-rao, DU Feng-guo. Extraction technology of anthocyanin from Lonicera caerulea 'Beilei' fruit by ultrasonic-assisted countercurrent extraction[J]. Journal of Beijing Forestry University, 2017, 39(9): 119-125. DOI: 10.13332/j.1000-1522.20170119
    Citation: ZHOU Li-ping, WANG Hua, HE Dan-rao, DU Feng-guo. Extraction technology of anthocyanin from Lonicera caerulea 'Beilei' fruit by ultrasonic-assisted countercurrent extraction[J]. Journal of Beijing Forestry University, 2017, 39(9): 119-125. DOI: 10.13332/j.1000-1522.20170119

    Extraction technology of anthocyanin from Lonicera caerulea 'Beilei' fruit by ultrasonic-assisted countercurrent extraction

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    • Received Date: April 06, 2017
    • Revised Date: June 17, 2017
    • Published Date: August 31, 2017
    • The response surface methodology based on single factor experiment was used to optimize processing parameters of extraction of Lonicera caerulea 'Beilei' anthocyanin by ultrasonic-assisted countercurrent extraction. The results showed that the optimal processing conditions of ultrasonic-assisted countercurrent extraction were ultrasonic time 28 min, extraction temperature 30 ℃ and ultrasonic power 120 W, the countercurrent extraction stage was three levels. The yields of anthocyanin under the optimal extraction conditions were up to (5.23±0.023) mg/g, the extraction rate was 99.80%, which was increased by 10% compared with ultrasonic extraction method. For the same batch of raw materials, compared with conventional ultrasonic extraction, this process can save three extraction solvent 67% and save time 44.4%.
    • [1]
      秦栋, 霍俊伟, 睢薇.蓝果忍冬品种蓓蕾蓝靛果引种与选育[J].中国果树, 2011 (5): 37-39.

      QIN D, HUO J W, SUI W. Introduction and breeding of Lonicera Caerulea Beilei[J]. China Fruits, 2011 (5): 37-39.
      [2]
      顾文秀, 谢为明, 夏文水, 等.超声波提取乌饭树叶色素及其稳定性的研究[J].林产化学与工业, 2005, 25 (4): 74-78. doi: 10.3321/j.issn:0253-2417.2005.04.018

      GU W X, XIE W M, XIA W S, et al. Ultrasonic extraction of pigment from leaves of Vaccinium bracteatum Thumb.[J]. Chemistry and Industry of Forest Products, 2005, 25 (4): 74-78. doi: 10.3321/j.issn:0253-2417.2005.04.018
      [3]
      时玉晴, 苏东民, 苏东海, 等.超声波辅助法提取黑色小麦麸皮花色苷工艺优化[J].粮食与油脂, 2015, 28(4): 15-18. doi: 10.3969/j.issn.1008-9578.2015.04.005

      SHI Y Q, SU D M, SU D H, et al. Optimization of extraction process for black wheat bran anthocyanins by ultrasonic-assisted extraction[J]. Grain and Oil, 2015, 28(4): 15-18. doi: 10.3969/j.issn.1008-9578.2015.04.005
      [4]
      程秀玮, 魏玮.响应面优化超声波辅助提取桑葚花色苷工艺的研究[J].中国酿造, 2014, 33 (6): 123-127. http://d.old.wanfangdata.com.cn/Periodical/zgnz201406030

      CHENG X W, WEI W. Optimization of ultrsonic extraction technology of melberry anthocyanin by response surface methodology[J]. China Brewing, 2014, 33 (6): 123-127. http://d.old.wanfangdata.com.cn/Periodical/zgnz201406030
      [5]
      李金星, 胡志和, 马立志, 等.超声波辅助提取蓝莓果渣中花色苷的条件研究[J].食品工业科技, 2013, 34 (20): 255-259. http://d.old.wanfangdata.com.cn/Periodical/spgykj201320058

      LI J X, HU Z H, MA L Z, et al. Study on conditions of anthocyanins from blueberry pomace by ultrasonic-assisted extraction[J]. Science and Technology of Food Industry, 2013, 34 (20): 255-259. http://d.old.wanfangdata.com.cn/Periodical/spgykj201320058
      [6]
      李希, 谢守德, 冯建安, 等.动态逆流提取技术在中药提取中的应用[J].实用中医药杂志, 2008, 24(12): 806-808. doi: 10.3969/j.issn.1004-2814.2008.12.050

      LI X, XIE S D, FENG J A, et al. Application of dynamic countercurrent extraction technology in extraction of traditional chinese medicine[J]. Journal of Practical Traditional Chinese Medicine, 2008, 24(12): 806-808. doi: 10.3969/j.issn.1004-2814.2008.12.050
      [7]
      张毅, 宁正祥, 董华强, 等.多穗柯总黄酮的连续逆流提取研究[J].现代食品科技, 2011, 27(5): 550-552, 570. http://d.old.wanfangdata.com.cn/Periodical/gzspgykj201105016

      ZHANG Y, NING Z X, DONG H Q, et al. Continuous countercurrent extraction of flavonoids from Lithocarpus polysachyus Rehd.[J]. Modern Food Science and Technology, 2011, 27(5): 550-552, 570. http://d.old.wanfangdata.com.cn/Periodical/gzspgykj201105016
      [8]
      王巧娥, 任虹, 曹学丽.甘草中甘草酸的多级逆流提取技术研究[J].北京工商大学学报(自然科学版), 2011, 29(1): 33-37. http://d.old.wanfangdata.com.cn/Periodical/bjqgyxyxb201101008

      WANG Q E, REN H, CAO X L. Multistage countercurrent extraction techniques for extraction of glycyrrhizic acid from licorice[J]. Journal of Beijing Technology and Business University(Natural Science Edition), 2011, 29(1): 33-37. http://d.old.wanfangdata.com.cn/Periodical/bjqgyxyxb201101008
      [9]
      栾连军, 陈娜, 刘雪松, 等.葡萄籽原花青素多级逆流提取工艺研究[J].中国食品学报, 2010, 10(5): 31-36. doi: 10.3969/j.issn.1009-7848.2010.05.005

      LUAN L J, CHEN N, LIU X S, et al. Studies on the multi-stage countercurrent extraction technology for the extraction of proanthocaynidins from grape seed[J]. Journal of Chinese Institute of Food Science and Technology, 2010, 10(5): 31-36. doi: 10.3969/j.issn.1009-7848.2010.05.005
      [10]
      韩丽, 谢秀琼, 杨明, 等.丹参动态阶段连续逆流提取工艺研究[J].中成药, 2009, 31(5): 721-724. doi: 10.3969/j.issn.1001-1528.2009.05.020

      HAN L, XIE X Q, YANG M, et al. Study on continuous extraction of Salvia miltiorrhiza[J]. Chinese Traditional Patent Medicine, 2009, 31(5): 721-724. doi: 10.3969/j.issn.1001-1528.2009.05.020
      [11]
      王艳艳, 王团结, 陈娟.连续动态逆流提取技术及其设备研究[J].机电信息, 2015(5): 1-9, 14. doi: 10.3969/j.issn.1671-0797.2015.05.001

      WANG Y Y, WANG T J, CHEN J. Study on continuous dynamic countercurrent extraction technology and equipment[J]. Electromechanical Information, 2015(5): 1-9, 14. doi: 10.3969/j.issn.1671-0797.2015.05.001
      [12]
      焦岩, 王振宇.蓝靛果花色苷对高脂膳食诱导肥胖大鼠脂代谢和抗氧化能力的影响[J].食品科学, 2010, 31(3): 230-234. http://d.old.wanfangdata.com.cn/Periodical/spkx201003053

      JIAO Y, WANG Z Y. Effect of Lonicera caerulea anthocyanin on lipid metabolism and antioxidant function in high fat diet-induced obese rats[J]. Food Science, 2010, 31(3): 230-234. http://d.old.wanfangdata.com.cn/Periodical/spkx201003053
      [13]
      ZHAO H T, WANG Z Y, MA F M, et al. Protective effect of anthocyanin from Lonicera caerulea var. edulis on radiation-induced damage in mice[J]. International Journal of Molecular Sciences, 2012, 13(9): 11773-11782. http://d.old.wanfangdata.com.cn/OAPaper/oai_doaj-articles_88d2239bb7a9e123238cc1e70313f610
      [14]
      王恩福, 包怡红.蓝靛果提取物调节血脂功能特性的研究[J].食品与机械, 2010, 26(1): 81-82. http://d.old.wanfangdata.com.cn/Periodical/spyjj201001023

      WANG E F, BAO Y H. Study on blood lipid adjusting effect of Lonicera edulis extracts[J]. Food & Machinery, 2010, 26(1): 81-82. http://d.old.wanfangdata.com.cn/Periodical/spyjj201001023
      [15]
      谢志鹏, 刘雪松, 陈勇, 等.动态罐组式逆流提取技术在中药生产中的应用研究进展[J].中国中药杂志, 2007, 32(10): 884-887. doi: 10.3321/j.issn:1001-5302.2007.10.003

      XIE Z P, LIU X S, CHEN Y, et al. Advances in studies on multi-stage countercurrent extraction technology in traditional Chinese medicine[J]. China Journal of Chinese Materia Medica, 2007, 32(10): 884-887. doi: 10.3321/j.issn:1001-5302.2007.10.003
      [16]
      蔡铭, 陈勇, 刘雪松, 等.丹参中丹参素四效逆流提取工艺的优化[J].中国中药杂志, 2006, 31(18): 1499-1502. doi: 10.3321/j.issn:1001-5302.2006.18.005

      CAI M, CHEN Y, LIU X S, et al. Optmizing process of four-effect countercurrent extraction of dan shen su from Salvia miltiorrhiza[J]. China Journal of Chinese Materia Medica, 2006, 31(18): 1499-1502. doi: 10.3321/j.issn:1001-5302.2006.18.005
      [17]
      周丽萍, 杨瑞华, 张悦.响应面法优化研磨珠辅助超声波萃取苹果多酚的工艺研究[J].食品工业科技, 2012, 33(21): 277-281. http://d.old.wanfangdata.com.cn/Periodical/spgykj201221081

      ZHOU L P, YANG R H, ZHANG Y. Optimization of apple polyphenols extraction with grind balls by response surface methodology[J]. Science and Technology of Food Industry, 2012, 33(21): 277-281. http://d.old.wanfangdata.com.cn/Periodical/spgykj201221081
      [18]
      陈钢, 黄立山, 徐静, 等.黑莓花色苷的超声波提取与抗氧化性活性研究[J].食品科学, 2012, 33(24): 117-121. doi: 10.7506/spkx1002-6630-201224024

      CHEN G, HUANG L S, XU J, et al. Ultrasonic-assisted extraction and antioxidant activity of anthocyanins from blackberry fruits[J]. Food Science, 2012, 33(24): 117-121. doi: 10.7506/spkx1002-6630-201224024
      [19]
      张帅, 张少平, 郑云云, 等.红凤菜花色苷三种提取方法的工艺优化和比较[J/OL].食品工业科技, 2017[2017-03-15].http://kns.cnki.net/kcms/detail/11.1759.TS.20170307.1418.016.html.

      ZHANG S, ZHANG S P, ZHENG Y Y, et al. Optimization and comparison of three extraction methods of anthocyanin from Gynura bicolor[J/OL]. Science and Technology of Food Industry, 2017[2017-03-15]. http://kns.cnki.net/kcms/detail/11.1759.TS.20170307.1418.016.html.
      [20]
      王巧娥, 任虹, 曹学丽.动态逆流提取技术及其在天然活性成分提取中的应用[J].安徽农业科学, 2011, 39(5): 2535-2537, 2540. doi: 10.3969/j.issn.0517-6611.2011.05.006

      WANG Q E, REN H, CAO X L. Dynamic countercurrent extraction technology and its application in extracting natural active constituents[J]Journal of Anhui Agricultural Sciences, 2011, 39(5): 2535-2537, 2540. doi: 10.3969/j.issn.0517-6611.2011.05.006
      [21]
      陈红专, 王曙宾, 高鹏, 等.人参超声逆流提取工艺研究[J].中草药, 2012, 43 (6): 1115-1117. http://d.old.wanfangdata.com.cn/Periodical/zcy201206019

      CHEN H Z, WANG S B, GAO P, et al. Study on ultrasound countercurrent extraction technology of Panax ginseng[J]. Chinese Traditional and Herbal Drugs, 2012, 43(6): 1115-1117. http://d.old.wanfangdata.com.cn/Periodical/zcy201206019
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